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Scanning electron microscope (SEM) FEI Inspect F50

Instrument

Scanning electron microscopy (SEM) is a powerful imaging technique to study the morphology (shape, size, particle arrangement, etc.), surface topology (relief, texture, etc.), and chemical composition (relative ratios of chemical elements from carbon to uranium) of a sample. The SEM uses a focused beam of high-energy electrons to generate a variety of signals at the surface of solid specimens revealing information about the sample. SEM is used to analyze a multitude of samples of all shapes, compositions and sizes for samples stable under high-vacuum conditions. SEM is a non-destructive analytical method for electrically conductive material. The study of insulting materials, on the other hand, requires extra step for sample preparation including the deposition of thin conductive layer (carbon or palladium alloy).

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FEI Inspect F50

Rates

LA-ICP_MS_Table_Rates.PNG

Applications​

An abnornally fast deterioration of concrete containing sulfide-bearing aggregates has been observed in the Trois-Rivières area (Qc, Canada). In this publication Mineralogical and chemical assessment of concrete damaged by the oxidation of sulfide-bearing aggregates: Importance of thaumasite formation on reaction mechanisms (Rodrigues et al., Cement and Concrete Research, 2012, 42, 1336) the researchers were able to identify and understand the degradation mechanisms involved when using sulfide-bearing aggregates.

The use of scanning electron microscopy (SEM) enabled the identification of secondary reaction products such as thaumasite (Ca3Si(CO3)(SO4)(OH)6•12(H2O) and ettringite, (Ca6Al2(SO4)3(OH)12•26(H2O) two minerals known to impair the longevity of concrete. 



Contact

Contact

Nicholas Larouche, PhD


418 656-2131 poste 408052

microlab-sem@fsg.ulaval.ca

Booking

Available soon

Sample preparation

Sample preparation is usually minimal but depending on the nature of the samples and the data required, extra preparation steps can be required. Most electrically insulating samples require a metallization process (deposition of a thin layer of conducting material). The choice of the conductive coating depends on the data to be acquired; carbon is used for Energy dispersive X-ray Spectroscopy (EDS) and Wavelength Dispersive X-ray Spectroscopy (WDS) SEM analyses while Au-Pd or Pt-Pd alloys are used for high resolution electron imaging applications

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