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Electron probe micro-analyzer (EPMA) CAMECA SX-100

Instrument

The electron probe micro-analyzer (EPMA), also known as microprobe, is a non-destructive method used to determine the chemical composition of solid samples. EPMA works by bombarding a micro-volume of a sample with a focused electron beam (typical energy = 5-30 keV) and collecting the X-ray photons thereby emitted by the various elemental species. Because the wavelengths of these X-rays are characteristic of the emitting species, the sample composition is determined by recording WDS spectra (Wavelength Dispersive Spectroscopy). The primary importance of an EPMA is the ability to acquire precise, quantitative elemental analyses (as low as 50 ppm) of the majority of the elements (from boron to plutonium) of a complex sample of very small spot sizes (1-2 µm). The spatial scale of analysis, combined with the ability to create detailed images of the sample, makes it possible to analyze a multitude of solid samples such as rocks and minerals, metals and alloys, glass, optical fibers, ceramics, semiconductor materials, concrete, cement. The electron microprobe is an automated instrument, enabling analysis, profiling or elemental mapping of solid samples.    ​

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CAMECA SX-100

User Fees


Catégories d'utilisateur

Horaire (<6h)

Forfait journalier (6-23h)

Traitement des données (heure)

Carbon coating (horaire)

Université Laval

85 $

510 $

80 $

80 $

Recherche universitaire - Organisation supportée par des fonds publics

140 $

840 $

130 $

130 $

Industrie

255 $

1530 $

240 $

240 $




Contact

Contact

Enzo Caraballo Rojas, PhD


418 656-2131 poste 405035

microlab-epma@fsg.ulaval.ca

Professeur


Prof. Georges Beaudoin


georges.beaudoin@ggl.ulaval.ca

Booking

Sample preparation

​Samples (solids, powders or liquids) require little or no preparation for analysis. To maximize analysis conditions, even though samples may be irregular in shape, the surface to be analyzed must be flat and even. Polishing the sample will ensure a surface suitable for analysis. 


Samples must meet certain conditions to ensure consistent results.


1. Solid

     - mirror-like polished surface

2. Thin blades

    - minimum thickness of 30 microns 

    - polished sections: maximum diameter (D) of 2.5 cm and maximum height (H) of 3 cm.  

3. Powders

     - encapsulated in a polished section

     - maximum diameter (D) of 2.5 cm and maximum height (H) of 3 cm.


For any other type of sample, please contact the instrument manager for details.

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